Hydrogen Production

High-purity hydrogen (95%-99%) is required for hydrodesulfurization, hydrogenation, hydrocracking, and petrochemical processes. Hydrogen, produced as a by-product of refinery processes (principally hydrogen recovery from catalytic reformer product gases), often is not enough to meet the total refinery requirements, necessitating the manufacturing of additional hydrogen or obtaining supply from external sources.

In steam-methane reforming, desulfurized gases are mixed with superheated steam (1,100°-1,600° F) and reformed in tubes containing a nickel base catalyst. The reformed gas, which consists of steam, hydrogen, carbon monoxide, and carbon dioxide, is cooled and passed through converters containing an iron catalyst where the carbon monoxide reacts with steam to form carbon dioxide and more hydrogen. The carbon dioxide is removed by amine washing. Any remaining carbon monoxide in the product stream is converted to methane.

Steam-naphtha reforming is a continuous process for the production of hydrogen from liquid hydrocarbons and is, in fact, similar to steam-methane reforming. A variety of naphthas in the gasoline boiling range may be employed, including fuel containing up to 35% aromatics. Following pretreatment to remove sulfur compounds, the feedstock is mixed with steam and taken to the reforming furnace (1,250°-1,500° F) where hydrogen is produced.

Feedstock

From

Process

Typical products – to – unit

Desufurized refinery gas

Various treatment units

Decomposition

  • Hydrogen To Processing
  • Carbon dioxide To Atmosphere
  • Carbon monoxide To Methane

The potential exists for burns from hot gases and superheated steam should a release occur. Inspections and testing should be considered where the possibility exists for valve failure due to contaminants in the hydrogen. Carryover from caustic scrubbers should be controlled to prevent corrosion in preheaters. Chlorides from the feedstock or steam system should be prevented from entering reformer tubes and contaminating the catalyst.